Chemistry 350 - Principles of Organic Chemistry I
Fall Semester 2015, Winona State University


Laboratory Schedule

Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed

Dates

Lab Activities

Aug 24, 25, 26

Lab grading.  Assignment of lab teams. Check in to lab supply drawers. Chapter 4

Team contribution surveys.

Aug 31 Sep 1, 2

Learning from Molecular Models I - Non-cyclic Alkanes

Sep 7, 8, 9

No Labs due to Labor Day holiday

Sep 14, 15, 16

Guidelines for pre-lab notes. Chapter 3

Learning from Molecular Models II - Cyclic Alkanes
Sep 21, 22, 23

Introduction to the lab. Safety rules - PowerPoint. Safety rules - pdf. Chapter 1

Guidelines for the in-lab notes and lab reports. Chapter 3

Expt 1. Preparation of 4-Acetylbiphenyl. C-13 NMR and Melting Point Determination  Chapter 14, 21.1-21.3, 22.1-22.3

Sep 28, 29, 30

Expt 2. Unknown Determination by NMR and IR Spectroscopy  Chapter 20-21.

Pre-lab lecture on IR Spectroscopy. PowerPoint

Oct 5, 6, 7

Learning from Molecular Models III - Enantiomers and Diastereomers
Oct 12, 13, 14
Expt 3. Mechanistic Study of the Halogenation of Primary, Secondary and Tertiary Alcohols 

Chapter 16.3-16.4, 19, 23.

Oct 19, 20, 21

Expt 4. Dehydrohalogenation of  2-Bromoheptane  Chapter 11, 12

Oct 26, 27, 28

Finish up experiment #4. Begin working on lab reports.

Nov 2, 3, 4

Expt 5. Preparation of 1,2-Dibromo-1,2-diphenylethane  Chapter 15

Nov 9, 10, 11

No Labs due to Veterans Day holiday

Nov 16, 17, 18

Expt 6.Reaction of 1,5-Cyclooctadiene with Excess Dichlorocarbene

Nov 23, 24, 25
No Labs due to Thanksgiving holiday

Nov 23 12:00 and Nov 24 2:00
Optional Extra Credit Activity - Participate in Dr. Hein's research on multiple choice testing. Part 1. (Extra Credit)
Nov 30 Dec 1, 2

Labs will start with Optional Extra Credit Activity - Participate in Dr. Hein's research on multiple choice testing. Part 2.

Check out and clean up lab and Final Exam review sessions