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Chapter references are to Techniques for the Organic Chem Lab by Gregory Friestad. |
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| Dates |
Lab Activities |
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Aug 22,23 |
Go over syllabi and guidelines for lab notebooks.
Assignment of lab teams. |
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Aug 29,30 |
Set up lab teams. Check in to lab supply drawers. |
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Sep 5,6 |
Safety rules - PowerPoint Safety rules - pdf Expt 1. Synthesis of Acetaminophen. Melting point determination. |
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Sep 12,13 |
Expt 2. Acid/Base Extraction. Part 1 Acid/Base Extraction |
| Sep 19,20 |
Expt 2. Acid/Base Extraction. Part 2. C-13 NMR and mp Determination |
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Sep 26,27 |
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Oct 3,4 |
No Lab Meetings - a recorded
lecture on 1H NMR spectroscopy will be provided |
| Oct
10,11 |
Expt
3 - Preparation of Naphthyl Butyl Ether |
| Oct
17,18 |
Pre-lab lecture on IR Spectroscopy. Expt
3 - Obtain IR and mp |
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Oct 24,25 |
Pre-lab lecture on Mass Spectrometry. Expt 3 - Obtain
NMR and GC-MS |
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Oct 31, Nov 1 |
Expt 4 - Halogenation of a
Ketone |
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Nov 7,8 |
Expt 5. Two Addition Reactions of 3-hexene |
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Nov 14,15 |
Finish up expt 5 if necessary. |
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Nov 21,22 |
No Labs - Thanksgiving |
| Nov
28,29 |
Check out and lab clean up. |