Chemistry 351, Spring Semester 2013, Winona State University, Dr. T. Nalli

Laboratory Schedule

Dates


Jan 14,15,16 Establishment of Teams. Check in to lab supply drawers. Safety Rules.
Jan 21,22,23 No Lab - MLK Day
Jan 28,29,30

Expt 1. Oxidation of 2-Pentanol

Feb 4,5,6

Finish up Expt 1.

Feb 11,12,13

 

Feb 18,19,20

Expt 2. Epoxidation of (E)-ethyl 3-phenylbut-2-enoate

Feb 25,26,27

Finish up Expt 2.

Mar 4,5,6

Expt 3. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR

Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction

Mar 11,12,13

Finish up Expt 3 and Molecular Modeling Worksheet.

Mar 18,19,20

No Labs - Spring Break

Mar 25,26,27

Expt 4. Friedel Crafts Acylation of Anisole

Apr 1,2,3

Expt 5. Part 1. Grignard Synthesis of 3-Methylbenzoic Acid

Apr 8,9

No Labs

Apr 10,15,16

Expt 5. Part 2. Preparation of DEET. VT NMR Study of Amide C-N Bond Rotation

Apr 17 WSU Ramaley Celebration of Research and Creative Scholarship
Apr 22,23,24

Expt 6. A Crossed Aldol Condensation. Preparation of Dibenzalacetone

Apr 29,30 May 1

Supply Drawer Check Out. Lab Clean Up.

Exam 4 Review Sessions.