Chemistry 351 - Principles of Organic Chemistry II
Spring Semester 2014, Winona State University, Dr. Thomas Nalli

Dates


Jan 14,15 Establishment of Teams. Check in to lab supply drawers. Safety Rules.
Jan 21,22 Expt 1. Oxidation of 2-Pentanol
Jan 28,29 Finish up Expt 1.
Feb 4,5 Expt 2. Epoxidation of (E)-ethyl 3-phenylbut-2-enoate
Feb 11,12

Finish up Expt 2.

Feb 18,19 Expt 3. Friedel Crafts Acylation; Preparation of 4-Methoxypropiophenone
Feb 25,26 Finish up Expt 3.

Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction
Mar 4,5

Finish up Molecular Models.

Expt 4. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR
Mar 11,12

No Labs - Spring Break

Mar 18,19 Finish up Expt 4.
Mar 25,26

Expt 5. Multistep Synthesis. Synthesis of the Mosquito Repellant DEET from 3-Bromotoluene.

Part 1. Grignard Synthesis of 3-Methylbenzoic Acid

Apr 1,2

Expt 5. Part 2. Preparation of DEET.

Apr 8,9

Expt 6. Synthesis of an Assigned Chalcone via a Crossed Aldol Condensation.

Apr 15,16 No Labs - WSU Ramaley Celebration of Research and Creative Scholarship
Apr 22,23

Finish up Expt 6.

Apr 29,30

Supply Drawer Check Out. Lab Clean Up.

Exam 4 Review Sessions.