Chemistry 351 - Principles of Organic Chemistry II
Spring Semester 2015, Winona State University, Dr. Thomas Nalli

Lab Schedule

Dates


Jan 13,14 Establishment of Teams. Check in to lab supply drawers. Safety Rules.

Expt 1. Oxidation of 2-Pentanol
Jan 20,21 Finish up Expt 1.
Jan 27,28 Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction
Feb 3.4 Expt 2. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR
Feb 10,11 Finish up Expt 2.
Feb 17,18 Expt 3. Friedel Crafts Acylation; Preparation of 4-Methoxypropiophenone 
Feb 24,25 Expt 4. Reactions of Benzenediazonium Salts: Preparation of 4-Iodonitrobenzene and an Azo Dye.
Mar 3,4

Finish up Expt 4 (if necessary).
Mar 10,11

No Labs - Spring Break

Mar 17,18

Expt 5. Multistep Synthesis. Synthesis of the Mosquito Repellant DEET from 3-Bromotoluene.

Part 1. Grignard Synthesis of 3-Methylbenzoic Acid

Mar 24,25 No Labs.

Mar 31, Apr 1

Expt 5. Part 2. Preparation of DEET.

Apr 7,8

Expt 6. Synthesis of an Assigned Chalcone via a Crossed Aldol Condensation.

Apr 14,15 No Labs - Ramaley Celebration of Research and Creative Scholarship
Apr 21,22

Finish up Expt 6.

Apr 28,29

Supply Drawer Check Out. Lab Clean Up.

Exam 4 Review Sessions.