Chemistry 351, Summer Session 2012, Winona State University, Dr. T. Nalli

Laboratory Schedule

Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed

6/18

Establishment of Teams. Check in to lab supply drawers. Safety Rules.

Expt 1. Oxidation of 2-Pentanol Chapter 13, 16.3-16.4.
6/21

Finish up Expt 1.

6/25

Expt 2. SN2 Synthesis of an Aromatic Ether. Chapter 6-7, 10, 15.

6/28

Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction

Expt 3. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR

7/2

Expt 4. Friedel Crafts Acylation of tert-Butylbenzene

7/5

Expt 5. Microwave Assisted Suzuki Coupling (A photocopy of the procedures will be provided in lecture.)

7/9

Expt 6. Part 1. Grignard Synthesis of 3-Methylbenzoic Acid

7/12

Expt 6. Part 2. Amine Acylation - Preparation of DEET
7/16 Expt 7. Dyes
7/19

No Lab - Lab quizzes for expts 3,5,6. Lab clean up and supply drawer checkouts.