Principles of Organic Chemistry I
- Dr. Tom Nalli
Chemistry 350, Fall Semester 2012, Winona State
University
Laboratory Schedule
Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed
|
Lab Days |
Lab Activities |
|
Aug 28, 29, 30
|
Introduction to the lab
(SLC 386). Safety rules.
Lab grading. Pre-lab assignments. Chapters 1 and 3 |
|
Sep 4, 5, 6
|
Expt 1.
Melting Point Determination Guidelines for in-lab notes and lab reports. |
|
Sep 11, 12, 13
|
Assignment of lab teams. Team contribution forms. Check in to lab supply drawers. Chapter 4 |
|
Sep 18, 19, 20 |
Expt 2. C-13 NMR of
Alkanes and Alkenes Chapter 21.1-21.3,
22.1-22.3 |
| Sep 25, 26, 27 |
Completion of Molecular Models II - Cyclic Alkanes |
|
Oct 2, 3, 4 |
Expt 3. Unknown Determination by NMR and IR Spectroscopy Chapter 20-21. Pre-lab lecture on IR Spectroscopy. PowerPoint |
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Oct 9, 10, 11
|
Learning from Molecular Models III - Enantiomers and Diastereomers |
| Oct 16, 24, 25 | No Labs |
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Oct 23, 17, 18
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Expt 4. SN2 Synthesis of an Aromatic Ether.Chapter 6-7, 10, 15. 19, 23. Establishment of new lab teams. |
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Oct 30, 31, Nov 1
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Expt 5. Dehydrohalogenation of 2-bromoheptane Chapter 11, 12 |
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Nov 6, 7, 8
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Expt 6. Preparation of 1,2-Dibromo-1,2-diphenylethane Chapter 15 |
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Nov 13, 14, 15
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Completion of Expt 6. Obtain mps. |
| Nov 20, 21, 22 |
No labs - Thanksgiving |
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Nov 27, 28, 29
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Expt 8. Benzylic Bromination with NBS Expt 8 info and data for Wed and Thur lab sections. Expt 8 info and data for the Tuesday lab section.
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| Dec 4, 5, 6 | Check out and clean up lab and Final Exam review sessions |