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Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed |
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Lab Days |
Lab Activities |
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Aug 27, 28, 29 |
Introduction to the lab (SLC
386). Safety rules. Lab grading. Pre-lab assignments.
Chapters 1 and 3 |
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Sep 3, 4, 5 |
Expt 1. Melting Point
Determination Guidelines for in-lab notes and lab reports. |
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Sep 10, 11, 12 |
Assignment of lab teams. Team contribution forms. Check in to lab supply drawers. Chapter 4 |
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Sep 17, 18, 19 |
Experiment
2. Preparation of 4-Acetylbiphenyl Chapter
21.1-21.3, 22.1-22.3
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| Sep 24, 25, 26 | |
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Oct 1, 2, 3 |
Expt 3. Unknown Determination by NMR and IR Spectroscopy Chapter 20-21. Pre-lab lecture on IR Spectroscopy. PowerPoint |
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Oct 8, 9, 10 |
Learning from Molecular Models III - Enantiomers and Diastereomers |
| Oct 15,
16, 17 |
Expt 4. Preparation of 2-Naphthyl Butyl Ether Chapter 6-7, 10, 15. 19, 23. |
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Oct 22, 23, 24 |
No Labs |
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Oct 29, 30, 31 |
Expt 5. Dehydrohalogenation of 2-bromoheptane Chapter 11, 12 |
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Nov 5, 6, 7 |
Expt 6. Preparation of 1,2-Dibromo-1,2-diphenylethane Chapter 15 |
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Nov 12, 13, 14 |
Completion of Expt 6. Obtain mps. |
| Nov 19, 20, 21 |
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Nov 26, 27, 28 |
No labs - Thanksgiving |
| Dec 3, 4, 5 |
Check out and clean up lab and Final Exam review sessions |