Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed |
||
Dates |
Lab Activities |
Chapter |
Aug 27, 30 |
Go over syllabi and guidelines for lab notebooks and
reports. Assignment of lab teams. Check in to lab supply
drawers. |
3-4 |
Sep 6, 10 |
Safety
rules - PowerPoint Safety rules - pdf Meltemp
Heating Curves - Use to determine heat settings |
1 14 |
Sep 13, 17 |
Learning
from Molecular Models I - Non-cyclic Alkanes Map of Tools in Avogadro Molecular Modeling Software |
|
Sep 20, 24 |
Learning from Molecular Models II - Cyclic Alkanes | |
Sep 27, Oct 1 |
|
10, 11, 12 |
Oct 4, 8 |
Expt 2. Acid/Base Extraction. Part 2. Mass Spectrometry and C-13 NMR |
7.1, 15 |
Oct 11, 15 |
Learning from Molecular Models III - Enantiomers and Diastereomers | |
Oct
18 |
No Lab |
10, 21 |
Oct
22, 25 |
Expt 3
- Preparation of Naphthyl Butyl Ether via Williamson
Ether Synthesis |
10, 21, 23 |
Oct 29, Nov 1 |
Expt 3 - Process data. Work on lab reports |
|
Nov 5, 8 |
Pre-lab lecture - Stereochemistry of E2 and E1 reactions. Bases used for E2 reactions. Bulky bases. Expt 4. Dehydrohalogenation of 2-Bromoheptane |
19 |
Nov 12 |
No Lab - Veterans
Day |
|
Nov 15, 19 |
Expt 5 - Determination of a liquid unknown by IR and NMR |
|
Nov 26, 29 |
18 | |
Dec
3, 6 |
Check out and clean up. |