Chemistry 350 - Principles of Organic Chemistry I
Fall Semester 2021, Winona State University


Laboratory Schedule

Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed


Dates

Lab Activities

Chapter

Aug 24,25,26

Go over syllabi and guidelines for lab notebooks. Assignment of lab teams.

Molecular Models I - Lewis structures, VSEPR theory, and molecular polarity

Molecular Models I - Worksheet

3-4

Aug 31,
Sep 1,2

Safety rules - PowerPoint  Safety rules - pdf

Check in to lab supply drawers.

Expt 1. Synthesis of Acetaminophen. Melting point determination.

1



14

Sep 7,8,9

Molecular Models II - Alkanes and Cycloalkanes

Sep 14,15,16

Expt 2. Acid/Base Extraction. Part 1 Acid/Base Extraction 10, 11, 12
Sep 21,22,23

Expt 2. Acid/Base Extraction. Part 2. C-13 NMR and mp Determination

7.1, 15

Sep 28,29,30

Molecular Models III - Enantiomers and Diastereomers

10, 21

Oct 5,6,7

No Lab Meetings - a recorded lecture on 1H NMR spectroscopy will be provided

Oct 12,13,14
Expt 3 - Preparation of Naphthyl Butyl Ether
10, 21, 23
Oct 19,20,21
Expt 3  - Obtain NMR, and mp data.
Powerpoint

Oct 26,27,28

Exam 2 Review Sessions


Nov 2,3,4

Expt 4. Reaction of 3-hexene with Br2/H2O 20

Nov 9,10,11

Finish up Expt 4 if necessary

Watch recorded lecture on IR spectroscopy

Nov 16,17,18

Expt 5. NBS Bromination of Cyclohexene

Nov 23,24,25

No Labs - Thanksgiving

18
Nov 30
Dec 1,2

Check out and lab clean up.