Principles of Organic Chemistry II Laboratory Schedule

Week of	Experiment and Reading Assignment (Pavia techniques are in the Signature Lab Series Lab Manual.)
1/11	Establishment of Teams. Check in to lab supply drawers. Safety Rules.
1/18	Expt 1. Melting Point Determination
1/25	Expt 2. Free Radical Halogenation
2/1	Finish up Expt 2. Exam 1 Review Sessions.
2/8	Expt 3. Examination of Diels-Alder Cycloaddition using Molecular Models
2/15	Expt 4. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR.
2/22	Finish up Expt 4. Establish new lab teams.
3/1	Expt 5. Electrophilic Aromatic Substitution. Friedel-Crafts Acylation Lab Manual # 17 - Expt 59
3/8	No Labs - Spring Break
3/15	Finish up Expt 5. Obtain spectra.
3/22	No Labs
3/29	Expt 6. Grignard Synthesis of 4-Fluorotriphenylmethanol Lab Manual # 18 - Expt 38a (with major modification!)
4/5	Finish up Expt 6 (if necessary) Expt 7. Synthesis using Organozinc Reagents. Lab Manual # 20 - Expt 61 (This lab did not make it into the newest edition of the lab manual, if you need a copy please see me.) Consult this table to find out your assigned starting materials for Expt 7
4/12	Finish up Expt 7. Attend WSU Research Celebration Symposium on Wednesday 4/14.
4/19	Expt 8. A Crossed Aldol Condensation. Preparation of Dibenzalacetone. Note: For this lab a lab report is not required. Instead you will hand in fully labeled spectra attached to your in-lab notes. The in-lab notes should conclude with a table that lists the mp and yield results of the experiment. Also, you will need to submit your product in a fully labeled 2x2" ziploc. One procedure note: use a mixture of 15 mL EtOH, 3 mL 10% NaOH, and 3 mL water for step 2 on p 52.
4/26	No Labs - Exam 4 Review Sessions.