Chemistry 427 - Topics in Instrumental Chemistry
| Date |
Chapter |
Topic |
PowerPoint File |
| 1/13 |
1 |
MS ionization methods and
analyzers |
MSIM.pptx |
| 1/15 |
1 |
MS isotopes |
MS isotopes.ppt |
| 1/22 |
1 |
MS molecular ions and deducing
molecular formula |
MS M MF.ppt |
| 1/27 |
1 |
Class canceled |
|
| 1/29 |
1 |
MS fragmentation patterns. |
MS Frag.ppt |
| 2/3 |
2 |
GC-MS. Unknown Determination | |
| 2/5 |
2 |
MS arrow pushing. GC-MS. Unknown Determination | |
| 2/10 |
2 |
IR (Problem Set #1 Due Date) | IR1b.ppt |
| 2/12 |
2 |
IR |
|
| 2/17 |
3 |
H NMR |
NMR1b.ppt |
| 2/24 |
3 |
H NMR (Problem Set #2 Due Date) | NMR2b.ppt |
| 2/26 |
3 |
H NMR | |
| 3/3 |
3 |
H NMR |
NMR3b.ppt |
| 3/5 |
1-3 |
Unknown Determination from MS, IR, and H NMR | |
| 3/17 |
1-3 |
Unknown Determination from MS, IR, and H NMR (Problem Set #3 Due Date) | |
| 3/19 |
3 |
H NMR - splitting by other
nuclei (D, F-19, C-13, P-31) |
|
| 3/24 |
Midterm Exam |
Chapters 1-3 |
|
| 3/26 |
1-4 |
C-13 NMR shifts. Unknown Determination. | |
| 3/31 |
3 |
H NMR - relationships and spin
systems |
http://wenku.baidu.com/view/3d6e2b7d27284b73f2425042 |
| 4/2 |
4 |
DEPT C-13 NMR - Unknown
Problem Solving from MS, IR, H NMR, and DEPT C-13 NMR |
|
| 4/7 |
4 |
Theory behind Multiple-pulse NMR expts - Relaxation mechanisms, the rotating frame of reference. (APT) | |
| 4/9 |
1-4 |
Theory behind Multiple-pulse
NMR expts - the Attached Proton Test (APT) (Problem Set #4 Due Date) |
|
| 4/14 |
5 |
2D NMR Interpretation - COSY |
|
| 4/16 |
5 |
2D NMR Interpretation - HMQC |
|
| 4/21 |
6 |
2D NMR Interpretation - HMBC | |
| 4/23 |
6 |
2D NMR 2D NMR Interpretation -
INADEQUATE, TOCSY |
|
| 4/28 |
6 |
2D NMR in Unknown Determination | |
| 4/30 |
Final Exam |
||
| 5/2 |
(Final Problem Set Due Date) |