| Dates |
|
| Jan 10,
11 |
Lab Check In, Safety
Orientation, Go over Syllabi, Set up teams |
| Jan 17, 18 |
Prep for Expt 1 - (1) Recrystallize
1 g of N-bromosuccinimide from water. A helpful video
can be found at https://www.youtube.com/watch?v=JsAId6aXUQw (2) Distill cyclohexane. |
| Jan 24,
25 |
Expt
1 - NBS Bromination of 2-Hexene |
| Jan 31, Feb 1 | Expt 1 - Trial 2 |
| Feb 7, 8 | Obtain HNMRs for Expt 1. Molecular modeling - The Diels Alder reaction. |
| Feb 14, 15 | Expt 1 - Follow up - NBS
Bromination of 1-hexene (Thur lab) or 3-hexene (Wed lab) |
| Feb 21, 22 | Expt 2 - Grignard Synthesis of Hex-2-yn-4-ol |
| Feb 28, 29 | Purification of Expt 2
Product. |
| Mar 13 Mar 14 |
Expt3 - Preparation of 1-bromo-2-hexene - Procedures provided in lab. No prelab required. |
| Mar 20 Mar 21 |
Expt3 - Preparation of
1-bromo-2-hexene - Procedures provided in lab. No prelab
required. Lab clean up. Help prep for Expt 4. |
| Mar 27, 28 | Expt 4
- Determination of Sterols in Dried Mushrooms. Part 1.
Extraction |
| Apr 3, 4 | Expt 4
- Determination of Sterols in Dried Mushrooms. Part 2.
Prep for GC/MS |
|
Apr 10, 11 |
Expt 4 - Work up Data |
| Apr 17, 18 | No labs - Attend Ramaley Celebration on 4/18 |
| Apr 24, 25 | Check Out and Clean Up - Final Exam Review |