Chemistry 351, Summer 2014, Winona State University, Dr. T. Nalli
Laboratory Schedule
| Dates |
|
| July 7 | Establishment
of Teams. Check in to lab supply drawers. Safety Rules. Lab lecture on NMR spectroscopy and use of Delta software. |
| July 8 | Expt 1.
Unknown Determination by NMR and IR Spectroscopy
|
| July 9 |
Expt 2. Radical Polymerization of Styrene |
| July 10 |
Finish up Expt 2. |
| July 14 |
Expt 3. Friedel Crafts Acylation |
| July 15 | Finish up Expt 3. Molecular Models Worksheet - The Diels-Alder Reaction |
| July 16 |
Expt 4. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride |
| July 17 |
Expt 4 continued. Obtain mps and spectra. |
| July 21 |
Expt 4 continued. Obtain 2-D NMR spectra and determine peak assignments and J values. |
| July 22 |
|
| July 23 |
Finish up Expt 5, part 1. |
| July 24 |
Expt 5. Part 2. Preparation of DEET. |
|
July 28 |
Finish up Expt 5, part 2. |
| July 29 |
|
| July 30 |
Finish up Expt 6. |
| July 31 |
|
| August 4 |
Expt 8. A Crossed Aldol Condensation. Preparation of Dibenzalacetone |
| August 5 |
Finish up Expt 8. |
| August 6 |
Lab clean up. |
| August 7 |
No Lab |