CHEM 351:
SUMMER 2016
LABORATORY
SCHEDULE
Dr.
Vincent Sichula, Winona State University
|
Week |
Date |
Experiment |
Handout |
|
1 |
June
13 |
Check
In and Safety |
|
|
1 |
June
14 |
LAB 1: Oxidation of 2-pentanol |
|
|
1 |
June
15 |
LAB 1: Continued: NMR spectra and
Refractive index |
|
|
1 |
June
16 |
LAB 2: SN2
Synthesis of an Aromatic Ether
|
|
|
2 |
June
20 |
Learning
from Molecular Models: The Diels-Alder Cycloaddition
Reaction |
|
|
2 |
June
21 |
LAB 3:
The Diels-Alder Cycloaddition Reaction of alpha-Phellandrene with Maleic
Anhydride |
Lab 3 |
|
2 |
June
22 |
LAB 3:
Characterization of Product by 2-D NMR |
|
|
2 |
June
23 |
LAB 3:
The 2-D NMR spectra and J values |
|
|
3 |
June
27 |
LAB 4:
Friedel-Craft Acylation of
Toluene |
|
|
3 |
June
28 |
LAB 4: Friedel-Craft
Acylation of Toluene: Continued |
|
|
3 |
June
29 |
LAB 5: The
Reaction of Benzenediazonium
Salts |
|
|
June
30 |
LAB 5: The
Reaction of Benzenediazonium
Salts: Continued |
|
|
|
4 |
July
04 |
NO LAB: Independence Day |
|
|
4 |
July
05 |
LAB 6: Mutiple
Synthesis: Synthesis of the Mosquito Repellant DEET
from 3-Bromotoluene PART 1: Grignard
Synthesis of 3-Methylbenzoic Acid |
|
|
4 |
July
06 |
LAB 6: PART 2: The Preparation of
DEET |
Lab 6-2 |
|
4 |
July
07 |
LAB 6: PART 2: Continued |
|
|
5 |
July
11 |
LAB 7: Synthesis of Dibenzalacetone by a
Crossed Aldol Condensation |
|
|
5 |
July
12 |
LAB 8: Organic
Dyes, Drs. Sichula and Nalli |
|
|
5 |
July
13 |
NO LAB: CHECK OUT |
|
|
5 |
July
14 |
NO LAB |
|
|
5 |
July
15 |
FINAL EXAM with
Dr. Nalli |
|