Principles
of Organic Chemistry I - Dr. Tom
Nalli
Chemistry 350, Fall Semester 2010, Winona State University
Laboratory Schedule
Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 2nd ed
|
Lab Days |
Lab Activities |
|
8/24
and 8/26 |
Establishment of teams and introduction to the lab (SLC 386). Check in to lab supply drawers. Safety Rules. Lab notebooks. Lab grading. |
|
8/31
and 9/2 |
Expt
1. Melting Point Determinations Discussion of guidelines for lab reports and team contribution forms. |
|
9/7
and 9/9 |
No Labs |
|
9/14
and 9/16 |
Expt 2. C-13 NMR of Alkanes and Alkenes Chapter 19.1-19.5, 19.13 |
| 9/21 and 9/23 | Expt 3. Unknown Determination by NMR and IR Spectroscopy Chapter 18-19. Expt 4. Resolution of Enantiomers, Chapters 8 and 14. |
|
9/28
and 9/30 |
Completion of Experiment 3. Cyclohexane modeling work sheets. |
|
10/5
and 10/7 |
Completion of Expt 4. |
|
10/12
and 10/14 |
Expt 5. Preparation of an alkyl bromide Chapter 7-8.
|
|
10/19
and 10/21 |
Expt 5. Preparation of an alkyl bromide Finish up and obtain NMR, GC-MS, and IR spectra of product. Chapters 11 and 20. |
|
10/26
and 10/28 |
No Labs. |
|
11/2
and 11/4 |
|
| 11/9 and 11/11 | No labs - Veterans Day |
|
11/16
and 11/18 |
Expt 7. Dehydrobromination of 1,2-Dibromo-1,2-diphenylethane. |
| 11/23 and 11/25 | No labs - Thanksgiving
|
|
11/30
and 12/2 |
Check
Out
|