Principles of Organic Chemistry I
- Dr. Tom Nalli
Chemistry 350, Fall Semester 2011, Winona State
University
Laboratory Schedule
Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed
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Lab Days |
Lab Activities |
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Aug 22, 23, 24 |
Establishment of teams and introduction to the lab (SLC 386). Check in to lab supply drawers. Safety Rules.
Lab notebooks. Lab grading. Chapter 1-4 |
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Aug 30, 31, Sep 1 |
Expt 1.
Melting Point Determination Discussion of guidelines for lab reports and team contribution forms. |
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Sep 6, 7, 8 |
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Sep 13, 14, 15 |
Expt 2. C-13 NMR of
Alkanes and Alkenes Chapter 21.1-21.3,
22.1-22.3 |
| Sep 20, 21, 22 |
Expt 3. Unknown Determination by NMR and IR Spectroscopy Chapter 20-21. Pre-lab lecture on proton NMR. |
|
Sep
27, 28, 29 |
Completion of Experiment 3. Obtain Proton NMR Spectra. Pre-lab lecture on IR Spectroscopy. |
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Oct 4, 5, 6 |
Learning from Molecular Models III - Enantiomers and Diastereomers |
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Oct 11, 12, 13 |
Expt 4. SN2 Synthesis of an Aromatic Ether.Chapter 6-7, 10, 15. |
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Oct 18, 19, 20 |
Completion of Expt 4. Finish up and obtain mp, NMR, and GC/MS of product. Chapter 19, 23. Pre-lab lecture on Mass Spectroscopy and GC-MS. Establishment of new lab teams. |
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Oct 25, 26, 27 |
Expt 5. Dehydrohalogenation of 2-bromoheptane Chapter 11, 12, 13. |
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Nov 1, 2, 3 |
Expt 6. Preparation of 1,2-Dibromo-1,2-diphenylethane Chapter 15 |
| Nov 8, 9, 10 |
Completion of Expt 6. Obtain proton NMR and mp. |
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Nov 15, 16, 17 |
Expt 7. Microwave-Assisted Hydration of an Alkyne |
| Nov 22, 23, 24 |
No labs - Thanksgiving |
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Nov 29, 30, Dec 1 |
Check out
and clean up lab. Attendance required. |