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Chapter references are to Mohrig, Hammond, & Schatz Techniques in Organic Chemistry, 3rd ed |
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| Dates |
Lab Activities |
Chapter |
|
Aug 27, 29 |
Go over syllabi and guidelines for lab notebooks and
reports. Assignment of lab teams. Check in to lab supply
drawers. |
3-4 |
|
Sep 3, 5 |
Safety
rules - PowerPoint Safety rules - pdf Meltemp
Heating Curves - Use to determine heat settings |
1 14 |
|
Sep 10, 12 |
Learning
from Molecular Models I - Non-cyclic Alkanes Map of Tools in Avogadro Molecular Modeling Software |
|
|
Sep 17, 19 |
Learning from Molecular Models II - Cyclic Alkanes | |
| Sep 24, 26 |
|
10, 11, 12 |
|
Oct 1, 3 |
Expt 2. Acid/Base Extraction. Part 2. Mass Spectrometry and C-13 NMR |
7.1, 15 |
|
Oct 8, 10 |
Learning from Molecular Models III - Enantiomers and Diastereomers | |
| Oct
15, 17 |
Expt 3 - Preparation of
Naphthyl Butyl Ether via Williamson Ether Synthesis |
10, 21 |
| Oct 22, 24 | Pre-lab
lecture on GC-MS Expt 3 - Obtain mp and GC-MS. Work on lab reports |
10, 21, 23 |
|
Oct 29, 31 |
Pre-lab
lecture on proton NMR Expt 3 - Obtain proton NMR. Work on
lab reports. |
Powerpoint |
|
Nov 5, 7 |
Prelab lecture on how to use Delta for HNMR
processing. Expt 4 -Preparation of a Bromohydrin. You will react cis-3-hexene with NBS/water to form 4-bromo-3-hexanol by adapting a published procedure: Porter, D. J.; Stewart, A. T.; Wigal, C. T. J. Chem. Educ. 1995, 72, 1039-1040. |
19 |
|
Nov 12, 14 |
Expt 5 -
Epoxidation of cis or trans 3-hexene You will use
procedure A in the reference available to WSU students at
https://pubs.acs.org/doi/pdf/10.1021/ed078p77. As in the
previous lab, plan on using the same number of moles of
3-hexene as the reference paper uses of their alkene
(anethole). |
|
|
Nov 19, 21 |
Prelab lecture on IR spectroscopy Finish up expts 4 and 5 if necessary. |
Powerpoint |
|
Nov 26, 28 |
No Labs - Thanksgiving |
18 |
| Dec
3, 5 |
Prelab ILL session on solving spectroscopy problems Check out and lab clean up. |
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