Chemistry 351, Spring Semester 2007, Winona State University, Dr. T. Nalli
Laboratory Schedule
| Week of | Lab Activities |
| 1/15 | No Lab |
| 1/22 |
Establishment of Teams. Introduction to the Lab. Check in to lab supply drawers. Safety Rules. Expt 1. Melting Point Determination Pavia - Technique 9 |
| 1/29 |
Expt 2. TLC Analysis of Analgesic Drugs Pavia - Expt 11 |
| 2/5 | Expt 3. Cyclopropanation using Dichlorocarbene Pavia - Expt 26 |
| 2/12 |
Expt 4. Oxidation of Borneol and Reduction of Camphor Pavia, Expt 35 |
| 2/19 |
Finish up Expt 4 |
| 2/26 |
Expt 5. Radical Polymerization. Polystyrene Pavia - Expt 49c,d (no report required) |
| 3/5 |
No Lab - Spring Break |
| 3/12 |
Establish new lab teams. Expt 6. Examination of Diels-Alder Cycloaddition using Molecular Models (no prelab plan required) |
| 3/19 |
Expt 7. Electrophilic Aromatic Substitution. Friedel-Crafts Acylation Pavia - Expt 59 |
| 3/26 |
Finish up Expt 7 (obtain spectra, write up short report - individual results and spectra). |
| 4/2 |
Expt 8. Grignard Synthesis of 4-Fluorotriphenylmethanol Pavia - Expt 38a |
| 4/9 | Finish up Expt
8.
Attend WSU Research Celebration - especially students presenting posters on organic chemistry research. SLC Atrium. |
| 4/16 | Expt 9. Synthesis of DEET and Variable Temperature NMR Study of Amide Bond Rotation Pavia - Expt 47 |
| 4/23 |
Expt 10. Knoevenagel Condensation. Synthesis of Coumarin Derivatives. |