Chemistry 351 - Principles of Organic Chemistry II
Spring Semester 2017, Winona State University, Dr. Thomas Nalli

Lab Schedule

Dates


Jan 9, 10
Establishment of Teams. Check in to lab supply drawers. Safety Rules. Lab notebooks.
Jan 16, 17
No Labs
Jan 23, 24
Expt 1. Oxidation of a Secondary Alcohol
Jan 30, Feb 1
Finish up Expt 1.
Feb 6, 7
Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction
Feb 13,14 Expt 2. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR
Feb 20, 21 Finish up Expt 2.
Feb 27, 28

No Labs
Mar 6, 7

Spring Break

Mar 13, 14 Expt 3. Friedel Crafts Acylation of Naphthalene
Mar 20, 21 Expt 4. TLC-MS Determination of Pigments in Dried Peppers

Mar 27, 28

Expt 5. Multistep Synthesis. Synthesis of the Mosquito Repellant DEET from 3-Bromotoluene.
Part 1. Grignard Synthesis of 3-Methylbenzoic Acid
Apr 3, 4
No Labs
Apr 10, 11 Expt 5. Part 2. Preparation of DEET.
Apr 17, 18
Expt 6. Preparation of Dibenzalacetone vial Aldol Condensation
Apr 24, 25

Supply Drawer Check Out. Lab Clean Up.

Exam 4 Review Sessions.