Dates |
|
Jan 9, 10 |
Establishment of Teams. Check in to lab supply drawers. Safety Rules. Lab notebooks. |
Jan 16, 17 |
No Labs |
Jan 23,
24 |
Expt 1. Oxidation of a Secondary Alcohol |
Jan 30,
Feb 1 |
Finish up Expt 1. |
Feb 6, 7 |
Learning from Molecular Models - The Diels-Alder Cycloaddition Reaction |
Feb 13,14 | Expt 2. Diels-Alder Reaction of alpha-Phellandrene with Maleic Anhydride. Characterization of Product by 2-D NMR |
Feb 20, 21 | Finish up Expt 2. |
Feb 27,
28 |
No Labs |
Mar 6, 7 |
Spring Break |
Mar 13, 14 | Expt 3. Friedel Crafts Acylation of Naphthalene |
Mar 20, 21 | Expt 4. TLC-MS Determination of
Pigments in Dried Peppers |
Mar 27, 28 |
Expt 5. Multistep
Synthesis. Synthesis of the Mosquito Repellant DEET from
3-Bromotoluene. Part 1. Grignard Synthesis of 3-Methylbenzoic Acid |
Apr 3, 4 |
No Labs |
Apr 10, 11 | Expt 5. Part 2. Preparation of DEET. |
Apr 17,
18 |
Expt 6. Preparation
of Dibenzalacetone vial Aldol Condensation |
Apr 24, 25 |
Supply Drawer Check Out. Lab Clean Up. Exam 4 Review Sessions. |