Chemistry 351, Summer 2019, Winona State University, Dr. T. Nalli
Laboratory Schedule
| Dates |
|
| July 8 |
Establishment of Teams. Check in to lab supply drawers. Safety Rules. Lab Notebooks. |
| July 9 |
Expt 1. Preparation of
Heptyl Bromide |
| July 10 |
Finish up Expt 1. Distillation. |
| July 11 |
Finish up Expt 1. Flash chromatography, GC-MS, NMR/Delta. |
| July 15 |
Expt 2. Grignard Synthesis of
8-Pentadecanol |
| July 16 |
Finish up Expt 2 |
| July 17 |
Expt
3. Diels-Alder Reaction of alpha-Phellandrene with
Benzoquinone Molecular Models Worksheet - The Diels-Alder Reaction |
| July 18 |
Expt 3. continued. Product
purification. Finish molecular modeling worksheet. |
| July 22 |
Expt 3. continued. Obtain spectra and mps. |
| July 23 |
Expt 4. Friedel Crafts Acylation
of Anisole |
| July 24 |
Finish up Expt 4 |
| July 25 |
Work on lab reports. |
|
July 29 |
|
| July 30 |
Finish up expt 6 |
| July 31 |
No Lab |
| Aug 1 |
Expt 7. A Crossed Aldol Condensation |
| Aug 5 |
|
| Aug 6 |
Lab clean up and check out. Lab quizzes. |