| Dates |
|
| Jan 9,
10, 11 |
Establishment of Teams.
Check in to lab supply drawers. Safety Rules. Lab
notebook and report expectations. |
| Jan 16, 17, 18 |
Expt 1. Oxidation of 2-Octanol |
| Jan 23,
24, 25 |
Finish up Expt 1. |
| Jan 30,
31, Feb 1 |
Learning from Molecular Models - The Diels-Alder Reaction |
| Feb 6, 7,
8 |
Expt
2. Diels-Alder Reaction of alpha-Phellandrene with
p-Benzoquinone; Introduction to 2D-NMR |
| Feb 13,
14, 15 |
Finish up Expt 2 |
| Feb 20,
21, 22 |
Expt 3. Friedel Crafts Acylation of Naphthalene |
| Feb 27,
28, Mar 1 |
Finish up Expt 3 |
| Mar 6, 7,
8 |
Spring Break |
| Mar 13,
14, 15 |
Expt 4. Green Wittig Synthesis;
Introduction to APCI-MS |
| Mar 20,
21, 22 |
Finish up Expt 4 |
|
Mar 27, 28, 29 |
Expt 5. Multistep
Synthesis. Synthesis of p-DEET from
4-Bromotoluene. Part 1. Grignard Synthesis of 4-Methylbenzoic Acid |
| Apr 3, 4,
5 |
Expt 5. Part 2. Preparation of
p-DEET |
| Apr 10,
11, 12 |
No labs. Attend Ramaley
Research Celebration on April 11. |
| Apr 17,
18, 19 |
Expt 6. Preparation
of Dibenzalacetone vial Aldol Condensation |
| Apr 24,
25, 26 |
Supply Drawer Check Out. Lab Clean Up. Exam 4 Review Sessions. |